The measurement of the Doppler broadening of annihilation
line is very popular and frequently use in the positron
annihilation studies. The typical setup consists with the
germanium detector, a positron source with sandwiched two
identical samples fixed in a holder. The setup requires
also a multichannel analyzer which collects the measured
spectrum.
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In this measurement we analyze the shape of the
annihilation line (511 keV) obtained for several samples.
Therefore we extract the so-called S-parameter which is
defined as the ratio of counts in the central part to
the total area of annihilation line. This parameter is
sensitive to the low momentum electrons which mainly are
present in the open volume defects. The increase of the
value of this parameter indicates the increase of the
number of these defects where positrons are localized.
It is well visible in the presented example where the
annihilation line measured for the well annealed and
exposed to the compression copper sample are depicted.
The sample after compression has visible more counts
in the central part. It is also useful to extract the
so-called wing W-parameter which is defined as the ratio
of counts in the off central part to the total area of
annihilation line. The W-parameter is more sensitive to
the chemical surrounding of annihilation site than the
S parameter, because core electrons having higher momenta
are contributing mainly to the region of larger energy
deviation from 511 keV.
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For the analysis of the annihilation line the SP has
been written. This program allows to extract the
the S-parameter and W-parameter after fitting the gauss
curve to the experimental points and subtraction of the
background. The maximum of this curve defines the 511 keV
position what is important for definition of regions for
integration procedure in the calculations of the S- and
W-parameters. The program is freeware.
Download: Instal-SP-1.ZIP (2 MB).
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